1: With borane-THF in tetrahydrofuran T=20°C; 2 h; 2: With sodium hydroxide; dihydrogen peroxide in diethyl ether 0.5 h; 3: With phosphorus tribromide in pentane 12 h; Heating; Title compound not separated from byproducts;
pyridine; phosphorus tribromide in Petroleum ether T=-10.1°C; 2 h;
参考文献
Davies, Alwyn G.; Griller, David; Ingold, Keith U.; Walton, John C.; Lindsay, David A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 633 - 641
Bloodworth, A. J.; Eggelte Henny J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 3272 - 3278
Jamieson, Campbell; Walton, John C.; Ingold, Keith U.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 1366 - 1371
4 h; Ambient temperatureIrradiationEffect of added t-butyl hypochlorite; Product distributionMechanism;
参考文献
Jamieson, Campbell; Walton, John C.; Ingold, Keith U.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 1366 - 1371
