2,4,6-三氯-5-丙烷-2-基嘧啶合成路线 （共 5 条）
反应条件
N,N-diethylaniline; trichlorophosphate T=140°C;
参考文献
Guo, Hongyan; Kim, Choung U.; Kim, Hae Soo; Lee, Chong-Kyo; Lee, Ill Young; Mitchell, Michael L.; Son, Jong Chan; Xu, Lianhong
Patent: US2008/70920 A1, 2008 ;
Location in patent: Page/Page column 117-118 ;
反应条件
N,N-diethylaniline; trichlorophosphate in water
参考文献
Sylachim
Patent: US6452006 B1, 2002 ;
反应条件
1: Na / methanol / Heating 2: 89 percent / POCl3, 2,6-lutidine / Heating View Scheme
参考文献
Al-Turkistani, Abdulghafoor A.; Al-Deeb, Omar A.; El-Brollosy, Nasser R.; El-Emam, Ali A.
Molecules, 2011 , vol. 16, # 6 p. 4764 - 4774
反应条件
1: 93 percent / tetrahydrofuran / -78 °C 2: 95 percent / NaOMe / 4 h / Heating 3: 85 percent / HCl / H2O / 3 h / Heating 4: 1) HMDS, Me3SiCl, 2) stannic chloride / 1) reflux, 2) CH3CN, room temperature, 10 h View Scheme
参考文献
Lee, Yeon Soo; Kim, Yong Hae
Synthetic Communications, 1999 , vol. 29, # 9 p. 1503 - 1517
反应条件
1: 93 percent / tetrahydrofuran / -78 °C 2: 95 percent / NaOMe / 4 h / Heating 3: 85 percent / HCl / H2O / 3 h / Heating View Scheme
参考文献
Lee, Yeon Soo; Kim, Yong Hae
Synthetic Communications, 1999 , vol. 29, # 9 p. 1503 - 1517
