2,4,6-三氯-5-甲基嘧啶合成路线 （共 15 条）
反应条件
trichlorophosphate in dichloromethane; N,N-dimethyl-aniline
参考文献
Ciba-Geigy Corporation
Patent: US4741760 A1, 1988 ;
反应条件
phosphoric acid; trichlorophosphate T=100°C; 0.75 h;
参考文献
Organic Letters, , vol. 9, # 9 p. 1639 - 1641
参考文献
Chemische Berichte, , vol. 38, p. 3397
反应条件
1: zinc dust; water 2: alcohol; ammonia / 200 °C / im Rohr View Scheme
参考文献
Gerngross
Chemische Berichte, 1905 , vol. 38, p. 3397
反应条件
1: alcoholic ammonia / 160 °C / im Rohr 2: concentrated hydriodic acid; red phosphorus View Scheme
参考文献
Gerngross
Chemische Berichte, 1905 , vol. 38, p. 3397
参考文献
Gerngross
Chemische Berichte, 1905 , vol. 38, p. 3397
参考文献
Gerngross
Chemische Berichte, 1905 , vol. 38, p. 3397
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane 36 h; Heating;
参考文献
Ye, Chengfeng; Gao, Haixiang; Boatz, Jerry A.; Drake, Gregory W.; Twamley, Brendan; Shreeve, Jean'ne M.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 43 p. 7262 - 7265
反应条件
1: alcohol; ammonia / 20 °C 2: phosphonium iodide; fuming hydriodic acid / 60 - 70 °C 3: zinc dust; water / Behandeln mit verd. Kalilauge View Scheme
参考文献
Gerngross
Chemische Berichte, 1905 , vol. 38, p. 3397
反应条件
methanol; palladium on activated charcoal; magnesium oxide Hydrogenation;
参考文献
Pfleiderer; Mosthaf
Chemische Berichte, 1957 , vol. 90, p. 738,745
