2,3,4,5-四氢苯并[f][1,4]氧氮杂卓合成路线 （共 5 条）
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran T=0°C; 24 h; Heating / reflux; 2: With sodium hydroxide; water in tetrahydrofuran
参考文献
Allison, Brett D.; Hack, Michael D.; Phuong, Victor K.; Rabinowitz, Michael H.; Rosen, Mark D.
Patent: US2005/38032 A1, 2005 ;
Location in patent: Page/Page column 21 ;
US 20050038032 A1
反应条件
1: H2 / Raney-Ni / methanol / 3 h 2: LiAlH4 / diethyl ether; benzene / 15 h / Heating View Scheme
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 7, p. 1208 - 1212
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 7, p. 1288 - 1292
反应条件
lithium aluminium tetrahydride in diethyl ether; benzene 15 h; Heating;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 7, p. 1208 - 1212
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 7, p. 1288 - 1292
反应条件
formic acid; acetic anhydride in ethyl acetate
参考文献
Takeda Chemical Industries, Inc.
Patent: US6534496 B1, 2003 ;
反应条件
formic acid; acetic anhydride; sodium hydrogencarbonate in dichloromethane; water
参考文献
Takeda Chemical Industries, Ltd.
Patent: US6319916 B1, 2001 ;
