2,2-二氯-3-甲基-丁烷合成路线 (共 15 条)
反应条件
18-crown-6 ether; potassium tert-butylate in Petroleum ether T=80°C; 6 h;
参考文献
Dehmlow, Eckehard V.; Lissel, Manfred
Liebigs Annalen der Chemie, 1980 , # 1 p. 1 - 13
反应条件
phosphorus pentachloride in pentane
T=45°C;
参考文献
Giumanni
Bollettino chimico farmaceutico, 1967 , vol. 106, # 4 p. 230 - 242
反应条件
hydrogenchloride in diethyl ether
336 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Stammann, Guenter; Griesbaum, Karl
Chemische Berichte, 1980 , vol. 113, # 2 p. 598 - 606
反应条件
hydrogenchloride in liquid sulphur dioxide
504 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Stammann, Guenter; Griesbaum, Karl
Chemische Berichte, 1980 , vol. 113, # 2 p. 598 - 606
反应条件
1: liq. HCl / 264 h / Ambient temperature
2: liq. HCl / 240 h / Ambient temperature
View Scheme
参考文献
Stammann, Guenter; Griesbaum, Karl
Chemische Berichte, 1980 , vol. 113, # 2 p. 598 - 606
反应条件
phosphorus pentachloride
参考文献
Behal
Bulletin de la Societe Chimique de France, 1887 , vol. <2>48, p. 25
反应条件
hydrogenchloride
264 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Stammann, Guenter; Griesbaum, Karl
Chemische Berichte, 1980 , vol. 113, # 2 p. 598 - 606
反应条件
hydrogenchloride
264 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Stammann, Guenter; Griesbaum, Karl
Chemische Berichte, 1980 , vol. 113, # 2 p. 598 - 606
反应条件
hydrogenchloride
240 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Stammann, Guenter; Griesbaum, Karl
Chemische Berichte, 1980 , vol. 113, # 2 p. 598 - 606
反应条件
hydrogenchloride
240 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Stammann, Guenter; Griesbaum, Karl
Chemische Berichte, 1980 , vol. 113, # 2 p. 598 - 606