(E)-1-(2-羟基-4,6-二甲氧基苯基)-3-苯基丙酮合成路线 (共 14 条)
反应条件
potassium hydroxide in methanol T=20°C; Claisen condensation; 24 h;
参考文献
Singh, Om V.; Muthukrishnan; Sunderavadivelu
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 12 p. 2575 - 2581
反应条件
potassium hydroxide in methanol
参考文献
Pouget, Christelle; Lauthier, Fabienne; Simon, Alain; Fagnere, Catherine; Basly, Jean-Philippe; Delage, Christiane; Chulia, Albert-Jose
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 24 p. 3095 - 3097
反应条件
1: potassium carbonate / acetone 2: potassium hydroxide / methanol / 12 h / 50 °C / |Inert atmosphere View Scheme
参考文献
Seo, Young Ho; Park, Sun You
Bulletin of the Korean Chemical Society, 2014 , vol. 35, # 4 p. 1154 - 1158
反应条件
1: 84 percent / pyridine / methanol; H2O / 12 h / Heating 2: 92 percent / thallium(III) p-tosylate / acetonitrile / 2 h / Heating View Scheme
参考文献
Singh, Om V.; Muthukrishnan; Sunderavadivelu
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 12 p. 2575 - 2581
参考文献
Geissman; Fukushima
Journal of the American Chemical Society, 1948 , vol. 70, p. 1686,1688
反应条件
air; methylene blue in methanol 86 h; Irradiationfurther solvents, influence of substituents; Product distributionMechanism;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 1511 - 1513
反应条件
hydrogen bromide in acetic acid Heating;
参考文献
Liu, Tao; Ying, Huazhou; Lin, Guan; Hu, Yongzhou
Synthetic Communications, 2008 , vol. 38, # 11 p. 1815 - 1821
反应条件
iodine in dimethyl sulfoxide T=120°C; 4 h;
参考文献
Liu, Man; Zhang, Ji; Yang, Jian; Yang, Bo; Cui, Wei
Journal of Chemical Research, 2014 , vol. 38, # 3 p. 134 - 136
反应条件
iodine in dimethyl sulfoxide T=150°C; 4 h; Inert atmosphere;
参考文献
Synthetic Communications, , vol. 39, # 16 p. 2935 - 2948
反应条件
dicyclohexyl-carbodiimide in methanol Irradiation;
参考文献
Tetrahedron Letters, , vol. 28, # 39 p. 4615 - 4616