二甲基2,3-氮丙啶二羧酸酯合成路线 （共 10 条）
反应条件
ammonia in acetonitrile
16 h; Ambient temperature;
参考文献
Bucciarelli, Maria; Forni, Arrigo; Moretti, Irene; Prati, Fabio; Torre, Giovanni
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 23 p. 3041 - 3046
反应条件
Rh2(Piv)4 in 1,2-dichloro-ethane
2 h; Inert atmosphereReflux;
参考文献
Qi, Xinxin; Jiang, Yaojia; Park, Cheol-Min
Chemical Communications, 2011 , vol. 47, # 27 p. 7848 - 7850
反应条件
1: p-NO2-benzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / -20 °C / Inert atmosphere
2: Rh2(Piv)4 / 1,2-dichloro-ethane / 2 h / Inert atmosphere; Reflux
View Scheme
参考文献
Qi, Xinxin; Jiang, Yaojia; Park, Cheol-Min
Chemical Communications, 2011 , vol. 47, # 27 p. 7848 - 7850
反应条件
1: pyridine / 3 h / 20 °C / Inert atmosphere
2: p-NO2-benzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / -20 °C / Inert atmosphere
3: [Rh2(trifluoroacetate)4] / 1,2-dichloro-ethane / 80 °C / Inert atmosphere
View Scheme
参考文献
Qi, Xinxin; Jiang, Yaojia; Park, Cheol-Min
Chemical Communications, 2011 , vol. 47, # 27 p. 7848 - 7850
反应条件
1: p-NO2-benzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / -20 °C / Inert atmosphere
2: Rh2(Piv)4 / 1,2-dichloro-ethane / 2 h / Inert atmosphere; Reflux
View Scheme
参考文献
Qi, Xinxin; Jiang, Yaojia; Park, Cheol-Min
Chemical Communications, 2011 , vol. 47, # 27 p. 7848 - 7850
反应条件
1: p-NO2-benzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / -20 °C / Inert atmosphere
2: Rh2(Piv)4 / 1,2-dichloro-ethane / 2 h / Inert atmosphere; Reflux
View Scheme
参考文献
Qi, Xinxin; Jiang, Yaojia; Park, Cheol-Min
Chemical Communications, 2011 , vol. 47, # 27 p. 7848 - 7850
反应条件
1: p-NO2-benzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / -20 °C / Inert atmosphere
2: Rh2(Piv)4 / 1,2-dichloro-ethane / 2 h / Inert atmosphere; Reflux
View Scheme
参考文献
Qi, Xinxin; Jiang, Yaojia; Park, Cheol-Min
Chemical Communications, 2011 , vol. 47, # 27 p. 7848 - 7850
反应条件
1: p-NO2-benzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / -20 °C / Inert atmosphere
2: Rh2(Piv)4 / 1,2-dichloro-ethane / 2 h / Inert atmosphere; Reflux
View Scheme
参考文献
Qi, Xinxin; Jiang, Yaojia; Park, Cheol-Min
Chemical Communications, 2011 , vol. 47, # 27 p. 7848 - 7850
反应条件
1: p-NO2-benzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / -20 °C / Inert atmosphere
2: Rh2(Piv)4 / 1,2-dichloro-ethane / 2 h / Inert atmosphere; Reflux
View Scheme
参考文献
Qi, Xinxin; Jiang, Yaojia; Park, Cheol-Min
Chemical Communications, 2011 , vol. 47, # 27 p. 7848 - 7850
反应条件
1: pyridine / 3 h / 20 °C / Inert atmosphere
2: p-NO2-benzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / -20 °C / Inert atmosphere
3: Rh2(Piv)4 / 1,2-dichloro-ethane / 2 h / Inert atmosphere; Reflux
View Scheme
参考文献
Qi, Xinxin; Jiang, Yaojia; Park, Cheol-Min
Chemical Communications, 2011 , vol. 47, # 27 p. 7848 - 7850
