2,3-二氢-1,3-二甲基-2-硫酮喹唑啉-4(1H)-酮合成路线 （共 11 条）
反应条件
in methanol T=50°C; 3 h;
参考文献
Yun, L. M.; Yangibaev, S.; Shakhidoyatov, Kh. M.; Alekseeva, V. Ya.; V'yunov, K. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 9 p. 1001 - 1003
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 9 p. 1236 - 1238
反应条件
in acetic acid T=100°C; 2 h;
参考文献
Yun, L. M.; Yangibaev, S.; Shakhidoyatov, Kh. M.; Alekseeva, V. Ya.; V'yunov, K. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 9 p. 1001 - 1003
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 9 p. 1236 - 1238
反应条件
1.1: 3 h / 150 °C / |Inert atmosphere; |Schlenk technique 2.1: potassium hydroxide / acetonitrile / 0.25 h / 20 °C / |Inert atmosphere; |Schlenk technique 2.2: 4 h / 65 °C / |Inert atmosphere; |Schlenk technique 3.1: acetonitrile / 20 °C / |Inert atmosphere; |Schlenk technique 4.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.17 h / -80 °C / |Inert atmosphere; |Schlenk technique 5.1: sulfur / tetrahydrofuran / 2.5 h / 20 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Makhloufi, Abdelaziz; Wahl, Michaela; Frank, Walter; Ganter, Christian
Organometallics, 2013 , vol. 32, # 3 p. 854 - 861
反应条件
1.1: potassium hydroxide / acetonitrile / 0.25 h / 20 °C / |Inert atmosphere; |Schlenk technique 1.2: 4 h / 65 °C / |Inert atmosphere; |Schlenk technique 2.1: acetonitrile / 20 °C / |Inert atmosphere; |Schlenk technique 3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.17 h / -80 °C / |Inert atmosphere; |Schlenk technique 4.1: sulfur / tetrahydrofuran / 2.5 h / 20 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Makhloufi, Abdelaziz; Wahl, Michaela; Frank, Walter; Ganter, Christian
Organometallics, 2013 , vol. 32, # 3 p. 854 - 861
反应条件
1: acetonitrile / 20 °C / |Inert atmosphere; |Schlenk technique 2: sodium hexamethyldisilazane / tetrahydrofuran / 0.17 h / -80 °C / |Inert atmosphere; |Schlenk technique 3: sulfur / tetrahydrofuran / 2.5 h / 20 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Makhloufi, Abdelaziz; Wahl, Michaela; Frank, Walter; Ganter, Christian
Organometallics, 2013 , vol. 32, # 3 p. 854 - 861
反应条件
in diethylene glycol dimethyl ether 22 h; Heating;
参考文献
Barbuch, Robert J.; Peet, Norton P.
Organic Mass Spectrometry, 1988 , vol. 23, p. 816 - 820
反应条件
1: 54 percent / concentrated ammonium hydroxyde / ethanol / Heating 2: 50 percent / bis-(2-methoxy-ethyl) ether / 22 h / Heating View Scheme
参考文献
Barbuch, Robert J.; Peet, Norton P.
Organic Mass Spectrometry, 1988 , vol. 23, p. 816 - 820
反应条件
1: sodium hexamethyldisilazane / tetrahydrofuran / 25 °C 2: sulfur / tetrahydrofuran / 2.5 h / 20 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Makhloufi, Abdelaziz; Wahl, Michaela; Frank, Walter; Ganter, Christian
Organometallics, 2013 , vol. 32, # 3 p. 854 - 861
反应条件
in N,N-dimethyl-formamide T=50°C;
参考文献
Yun, L. M.; Yangibaev, S.; Shakhidoyatov, Kh. M.; Alekseeva, V. Ya.; V'yunov, K. A.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 11.2 p. 2196 - 2200
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 11 p. 2438 - 2444
反应条件
in N,N-dimethyl-formamide T=50°C;
参考文献
Yun, L. M.; Yangibaev, S.; Shakhidoyatov, Kh. M.; Alekseeva, V. Ya.; V'yunov, K. A.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 11.2 p. 2196 - 2200
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 11 p. 2438 - 2444
