(S)-2-苄氧基羰基氨基-1,4-双(甲烷磺酰氧基)丁烷合成路线 （共 4 条）
反应条件
triethylamine in ethyl acetate T=-20 - -5°C; 1 h;
参考文献
Tomori, Hiroshi; Shibutani, Kuniko; Ogura, Katsuyuki
Heterocycles, 1997 , vol. 44, # 1 p. 213 - 225
反应条件
1: 11.9 g / NaBH4 / tetrahydrofuran; methanol / 45 - 55 °C 2: 16.9 g / Et3N / ethyl acetate / 1 h / -20 - -5 °C View Scheme
参考文献
Tomori, Hiroshi; Shibutani, Kuniko; Ogura, Katsuyuki
Heterocycles, 1997 , vol. 44, # 1 p. 213 - 225
反应条件
1: 33.2 g / 1N HCl / Ambient temperature 2: 11.9 g / NaBH4 / tetrahydrofuran; methanol / 45 - 55 °C 3: 16.9 g / Et3N / ethyl acetate / 1 h / -20 - -5 °C View Scheme
参考文献
Tomori, Hiroshi; Shibutani, Kuniko; Ogura, Katsuyuki
Heterocycles, 1997 , vol. 44, # 1 p. 213 - 225
反应条件
1: 2.60 g / 3 h / 40 °C 2: 92 percent / AcOH / 10percent Pd/C / H2O / 1.5 h / 100 °C View Scheme
参考文献
Tomori, Hiroshi; Shibutani, Kuniko; Ogura, Katsuyuki
Heterocycles, 1997 , vol. 44, # 1 p. 213 - 225
