4-苯基硫代吗啉-1,1-二氧化物合成路线 （共 9 条）
反应条件
boric acid; glycerol in water T=100°C; Michael Addition; 18 h; Green chemistry;
参考文献
Halimehjnai, Azim Ziyaei; Hosseyni, Seyedmorteza; Gholami, Hadi; Hashemi, Mohammed M.
Synthetic Communications, 2013 , vol. 43, # 2 p. 191 - 197,7
参考文献
Journal of the American Chemical Society, , vol. 42, p. 1219,1220
反应条件
indium; ammonium chloride; acetic acid in methanol; water aza-Michael type 1,4-addition reaction; 24 h; Inert atmosphereReflux;
参考文献
Heterocycles, , vol. 81, # 2 p. 317 - 327
反应条件
sodium hydroxide; sodium tetrahydroborate; mercury(II) diacetate 1.) THF, 8 h, 2.) THF, 21 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Synthesis, , # 5 p. 417 - 419
反应条件
sodium cyanoborohydride; ozone; acetic acid 1.)MeOH, CH2Cl2; -60 deg C; 2.) MeOH, -60 deg C, 10 min; 0 deg C for 20 h; Yield given. Multistep reaction;
参考文献
Agricultural and Biological Chemistry, , vol. 51, # 2 p. 435 - 440
参考文献
Ricerca Scientifica, , vol. 22, p. 1589,1591
反应条件
hydrogenchloride; sodium nitrite Erwaermen des Reaktionsprodukts mit wss. NaOH;
参考文献
Ford-Moore
Journal of the Chemical Society, 1949 , p. 3433,3439
反应条件
1: With trichlorophosphate T=35 - 90°C; 4 h; 2: With ammonia; water T=0°C;
参考文献
US2006/115516 A1, ;
Page/Page column 25 ;
反应条件
diisobutylaluminium hydride in toluene
3.5 h; Heating;
参考文献
Kawaguchi, Mamoru; Hayashi, Osamu; Kanamoto, Masahiro; Hamada, Masayuki; Yamamoto, Yukio; Oda, Jun'ichi
Agricultural and Biological Chemistry, 1987 , vol. 51, # 2 p. 435 - 440
