反应条件
1.1: 93 percent / pyridine / 1.5 h / 20 °C
2.1: trimethylsilyl chloride; triethylamine / acetonitrile / -10 - 0 °C
2.2: 1,2,4-triazole; phosphorous oxycloride / acetonitrile / -20 - 0 °C
2.3: 85 percent / aq. ammonium hydroxide / dioxane / 1 h
View Scheme
参考文献
Ross, Bruce; Han, Mingming; Ravikumar, Vasulinga
Nucleosides, Nucleotides and Nucleic Acids, 2006 , vol. 25, # 7 p. 765 - 770