2-氨基-3-羟基苯甲酸甲酯合成路线 (共 20 条)
反应条件
palladium 10 on activated carbon; hydrogen in methanol T=20°C; 2 h; Inert atmosphere;
参考文献
Journal of Medicinal Chemistry, , vol. 56, # 8 p. 3310 - 3317
反应条件
1: in methanol; diethyl ether; toluene T=0°C; 0.333333 h; 2: With acetic acid in methanol; diethyl ether; toluene T=0 - 20°C; 0.5 h;
参考文献
US2008/214601 A1, ;
Page/Page column 22 ;
参考文献
Journal of the Chemical Society, , p. 980,984
Journal of Biological Chemistry, , vol. 196, p. 185,186
反应条件
hydrogenchloride 12 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 27, # 2 p. 335 - 336
反应条件
in methanol; diethyl ether T=0°C; 2 h;
参考文献
Journal of Medicinal Chemistry, , vol. 51, # 23 p. 7344 - 7347
反应条件
in methanol; diethyl ether T=0°C;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 14, # 17 p. 6106 - 6119
反应条件
potassium carbonate in dimethyl sulfoxide Methylation; 0.5 h;
参考文献
Tetrahedron, , vol. 56, # 46 p. 9057 - 9062
参考文献
Heterocycles, , vol. 64, p. 193 - 198
反应条件
1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 2 h / 40 °C / |Inert atmosphere 2: palladium 10 on activated carbon; hydrogen / methanol / 2 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 56, # 8 p. 3310 - 3317
反应条件
1: aqueous HCl 2: methanol. HCl View Scheme
参考文献
Journal of the Chemical Society, , p. 980,984