(S)-(+)-4-甲基-1-己醇合成路线 (共 27 条)
反应条件
lithium aluminium tetrahydride; diethyl ether Heating;
参考文献
Kelly, Stephen M.; Buchecker, Richard
Helvetica Chimica Acta, 1988 , vol. 71, p. 451 - 460
反应条件
lithium aluminium tetrahydride in diethyl ether 1 h; Ambient temperature;
参考文献
Kang, Suk-Ku; Lee, Dong-Ha; Sim, Hyeong-Su; Lim, Jong-Suk
Tetrahedron Letters, 1993 , vol. 34, # 1 p. 91 - 94
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 1 h;
参考文献
Ishmuratov; Yakovleva; Ganieva; Amirkhanov; Tolstikov
Chemistry of Natural Compounds, 2005 , vol. 41, # 6 p. 719 - 721
反应条件
ethanol; sodium; toluene
参考文献
Journal of Biological Chemistry, , vol. 95, p. 15
反应条件
1.1: NaH / ethanol / 1 h 1.2: 77 percent / ethanol / Heating 2.1: 78 percent / aq. LiCl / 4 h / Heating 3.1: LiAlH4 / diethyl ether / 1 h / 20 °C View Scheme
参考文献
Journal of Natural Products, , vol. 67, # 3 p. 395 - 401
反应条件
1: 78 percent / aq. LiCl / 4 h / Heating 2: LiAlH4 / diethyl ether / 1 h / 20 °C View Scheme
参考文献
Journal of Natural Products, , vol. 67, # 3 p. 395 - 401
反应条件
1: 57 percent / Br2; PPh3; imidazole / CH2Cl2 2: NaOEt / ethanol / Heating 3: KOH / methanol / Heating 4: 4 h / 190 °C 5: 86 percent / LiAlH4 / diethyl ether View Scheme
参考文献
European Journal of Organic Chemistry, , # 2 p. 353 - 363
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Journal of the American Chemical Society, , vol. 81, p. 2789,2794
反应条件
1: acetic acid; ozone / und Behandeln des Reaktionsgemisches mit wss.Eisen(II)-sulfat-Loesung 2: sodium borate View Scheme
参考文献
Journal of the American Chemical Society, , vol. 81, p. 2789,2794
反应条件
1: hydrazine hydrate; diethylene glycol / und Erhitzen des Reaktionsgemisches mit Kaliumhydroxid auf 170grad 2: acetic acid; ozone / und Behandeln des Reaktionsgemisches mit wss.Eisen(II)-sulfat-Loesung 3: sodium borate View Scheme
参考文献
Journal of the American Chemical Society, , vol. 81, p. 2789,2794