(R)-(-)-2-甲氧基-2-苯乙醇合成路线 (共 46 条)
反应条件
tin(IV) chloride T=-30°C; 0.5 h; other catalysts, variation of condition; Product distribution;
参考文献
Tetrahedron Letters, , vol. 33, # 16 p. 2191 - 2194
反应条件
immobilized Candida antarctica Lipase B T=30°C; 0.5 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 13, # 10 p. 1091 - 1096
反应条件
silica gel; iron (III) perchlorate T=20°C; Title compound not separated from byproducts;
参考文献
Russian Journal of Organic Chemistry, , vol. 39, # 6 p. 794 - 796
反应条件
1: poly((R)-2,2'-dihydroxy-5,5'-dicarboxy-1,1'-binaphthalene-copper complex) / 24 h / 40 °C / Resolution of racemate 2: poly((R)-2,2'-dihydroxy-5,5'-dicarboxy-1,1'-binaphthalene-copper complex) / 24 h / 40 °C View Scheme
参考文献
New Journal of Chemistry, , vol. 34, # 11 p. 2389 - 2391
反应条件
sodium tetrahydroborate; iodine; sodium hydrogencarbonate 1.) dioxan, water, room temperature, 20 min, 2.) 0 deg C; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1278 - 1283
反应条件
2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium chlorite in phosphate buffer; acetonitrile T=55°C; 4 h;
参考文献
Moreno-Dorado, F. Javier; Guerra, Francisco M.; Ortega, Maria J.; Zubia, Eva; Massanet, Guillermo M.
Tetrahedron Asymmetry, 2003 , vol. 14, # 4 p. 503 - 510