2-(2-丙基)-1,3-苯并噻唑合成路线 （共 24 条）
反应条件
2-iodobenzothiazole in dimethyl sulfoxide
Irradiation (UV/VIS); mercurial and organic compound dissolved in nitrogen purged solvent, irradn. (350-nm Rayonet photoreactor, 35-40°C, 22h);; mixt. poured into water; extn. with benzene; ext. washed (aq. Na2S2O3), dried (Na2SO4) and concd. (vacuum); yield detd. by (1)H NMR;;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.; Pla-Dalmau, Anna; Khanna, Rajive K.
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3530 - 3538
反应条件
in dimethyl sulfoxide
T=35 - 40°C; 24 h; Irradiation;
参考文献
Russell, Glen A.; Tashtoush, Hasan; Ngoviwatchai, Preecha
Journal of the American Chemical Society, 1984 , vol. 106, # 16 p. 4622 - 4623
反应条件
in dimethyl sulfoxide
T=35 - 40°C; 38 h; Irradiation;
参考文献
Russell, Glen A.; Tashtoush, Hasan; Ngoviwatchai, Preecha
Journal of the American Chemical Society, 1984 , vol. 106, # 16 p. 4622 - 4623
反应条件
dipotassium peroxodisulfate; silver nitrate in dichloromethane; water
T=20°C; 8 h;
参考文献
Zhao, Wei-Ming; Chen, Xiao-Lan; Yuan, Jin-Wei; Qu, Ling-Bo; Duan, Li-Kun; Zhao, Yu-Fen
Chemical Communications, 2014 , vol. 50, # 16 p. 2018 - 2020
反应条件
water; toluene-4-sulfonic acid
T=20°C; 16 h; Sealed tube;
参考文献
Mayo, Muhammad Shareef; Yu, Xiaoqiang; Zhou, Xiaoyu; Feng, Xiujuan; Yamamoto, Yoshinori; Bao, Ming
Organic Letters, 2014 , vol. 16, # 3 p. 764 - 767
反应条件
NiBr2(DMSO)PMe3 in tetrahydrofuran
3 h;
参考文献
Babudri, F.; Florio, S.; Ronzini, L.; Aresta, M.
Tetrahedron, 1983 , vol. 39, # 9 p. 1515 - 1521
反应条件
sodium dithionite in dimethyl sulfoxide
T=80°C; 10 h; Molecular sieve;
参考文献
Wang, Zhanglin; Tang, Riyuan; Xiao, Qin
Chinese Journal of Chemistry, 2011 , vol. 29, # 2 p. 314 - 320
反应条件
in dimethylsulfoxide-d6; dichloromethane
T=35 - 40°C; 22 h; Irradiation;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.; Pla-Dalmau, Anna; Khanna, Rajive K.
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3530 - 3538
反应条件
T=240°C; P=12928.7 Torr; 0.0666667 h; microwave irradiation;
参考文献
Kamila, Sukanta; Zhang, Hongming; Biehl, Edward R.
Heterocycles, 2005 , vol. 65, # 9 p. 2119 - 2126
反应条件
dibenzoyl peroxide; iron(III) cation in acetonitrile
T=80°C; Yield given;
参考文献
Castaldi, Graziano; Minisci, Francesko; Tortelli, Vito; Vismara, Elena
Tetrahedron Letters, 1984 , vol. 25, # 35 p. 3897 - 3900
