2,3-环氧-1,2,3,4-四水蒽合成路线 （共 5 条）
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform Ambient temperature;
参考文献
Dehaen, Wim; Corens, David; L'Abbe, Gerrit
Synthesis, 1996 , # 2 p. 201 - 203
反应条件
1: 70 percent / NaHCO3 / toluene / 36 h / 145 °C 2: 91 percent / conc. HCl / methanol / 15 h / Heating 3: 81 percent / MCPBA / CHCl3 / Ambient temperature View Scheme
参考文献
Dehaen, Wim; Corens, David; L'Abbe, Gerrit
Synthesis, 1996 , # 2 p. 201 - 203
反应条件
1: 91 percent / conc. HCl / methanol / 15 h / Heating 2: 81 percent / MCPBA / CHCl3 / Ambient temperature View Scheme
参考文献
Dehaen, Wim; Corens, David; L'Abbe, Gerrit
Synthesis, 1996 , # 2 p. 201 - 203
反应条件
1: 1.) CuI / 1.) Et2O, -10 deg C, 20 min, 2.) Et2O, 0 deg C, 1 h 2: 68 percent / o-chloranil / toluene / Heating View Scheme
参考文献
Dehaen, Wim; Corens, David; L'Abbe, Gerrit
Synthesis, 1996 , # 2 p. 201 - 203
反应条件
1: 1.) CuI / 1.) THF, -15 deg C, 5 min, 2.) THF, RT, 24 h 2: 61 percent / o-chloranil / toluene / Heating View Scheme
参考文献
Dehaen, Wim; Corens, David; L'Abbe, Gerrit
Synthesis, 1996 , # 2 p. 201 - 203
