4,4'-二氯-2,2'-联吡啶合成路线 （共 20 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride; tetrabutyl ammonium fluoride; silver(l) oxide in N,N-dimethyl-formamide T=90°C; 3 h; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 6 p. 1768 - 1773
反应条件
bis-triphenylphosphine-palladium(II) chloride; tetrabutyl ammonium fluoride; silver(l) oxide in N,N-dimethyl-formamide T=90°C; 3 h; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 6 p. 1768 - 1773
反应条件
phosphorus trichoride in acetonitrile 1) reflux, 1.75 h, 2) room temperature, overnight;
参考文献
Journal of Organic Chemistry, , vol. 48, # 3 p. 283 - 289
反应条件
bis-triphenylphosphine-palladium(II) chloride; tetrabutyl ammonium fluoride; silver(l) oxide in N,N-dimethyl-formamide T=90°C; 3 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 6 p. 1768 - 1773
反应条件
tetrakis(triphenylphosphine) palladium(0); silver fluoride; silver(l) oxide in N,N-dimethyl-formamide T=90°C; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 6 p. 1768 - 1773
反应条件
potassium fluoride; tetrakis(triphenylphosphine) palladium(0); silver(l) oxide in N,N-dimethyl-formamide T=90°C; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 6 p. 1768 - 1773
反应条件
trichlorophosphate 5 h; Heating;
参考文献
Tetrahedron, , vol. 39, # 2 p. 291 - 296
反应条件
potassium permanganate; sulfuric acid; water
参考文献
Haginiwa
Yakugaku Zasshi, 1955 , vol. 75, p. 733,735
Chem.Abstr., 1956 , p. 3436
反应条件
ammonia in various solvent(s) T=160°C; 24 h;
参考文献
Araki, Koji; Mutai, Toshiki; Shigemitsu, Yasuhiro; Yamada, Masaki; Nakajima, Takayoshi; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1996 , # 4 p. 613 - 618
反应条件
T=200 - 220°C; 90 h; Sealed tubeInert atmosphereSchlenk technique;
参考文献
Ladouceur, Sebastien; Swanick, Kalen N.; Gallagher-Duval, Shawn; Ding, Zhifeng; Zysman-Colman, Eli
European Journal of Inorganic Chemistry, 2013 , # 30 p. 5329 - 5343
