2,4-二氯-5-甲基苯胺合成路线 （共 7 条）
反应条件
1: hydrochloric acid; sodium chlorate 2: hydrochloric acid View Scheme
参考文献
Reverdin; Crepieux
Chemische Berichte, 1900 , vol. 33, p. 2505
反应条件
carbon disulfide; sulfuryl dichloride und Erwaermen des Reaktionsprodukts mit wss.Salzsaeure;
参考文献
Silvester; Wynne
Journal of the Chemical Society, 1936 , p. 691,694
反应条件
1: Diazotization.Behandlung der Diazoniumloesung mit CuCl 2: bei der Reduktion View Scheme
参考文献
Cohen; Dakin
Journal of the Chemical Society, 1902 , vol. 81, p. 1335
Journal of the Chemical Society, 1906 , vol. 89, p. 1454
参考文献
Cohen; Dakin
Journal of the Chemical Society, 1902 , vol. 81, p. 1335
Journal of the Chemical Society, 1906 , vol. 89, p. 1454
参考文献
Kalle and Co.
Patent: DE246265 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 10, p. 500
反应条件
1: 2,4-dichloro-5-methyl-aniline With hydrogenchloride in water
T=20°C;
2: With sodium nitrite in water
T=-5 - 0°C; 1.25 h;
3: [14C]-1,1-Dichloroethylene With copper dichloride in water; acetone
T=0 - 20°C;
参考文献
Bayer CropScience AG
Patent: US2010/234651 A1, 2010 ;
Location in patent: Page/Page column 3 ;
反应条件
Austausch von NH2 gegen Chlor;
参考文献
Cohen; Dakin
Journal of the Chemical Society, 1902 , vol. 81, p. 1335
Journal of the Chemical Society, 1906 , vol. 89, p. 1454
