反应条件
in carbon disulfide
byproducts: I2; addn. of KI to a soln. of SCl2 and Se2Cl2 in CS2 and stirring at 20°C for 4 h under exclusion of light, further products; filtn. of the reaction mixt., and shaking the filtrate with Na2S2O3*5H2O for 5 min (removal of I2), filtn. of the mixt. again and drying the filtrate with MgSO4, crystn. of orange needles covered with dark red grains after 24 h at -78°C, HPLC;
参考文献
Steudel, Ralf; Strauss, Eva-Maria
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1983 , vol. 38, # 6 p. 719 - 725