4-羟基-7-甲氧基香豆酯合成路线 （共 31 条）
反应条件
sodium hydride in mineral oil T=0 - 100°C;
参考文献
Nolan, Karen A.; Doncaster, Jeremy R.; Dunstan, Mark S.; Scott, Katherine A.; Frenkel, A. David; Siegel, David; Ross, David; Barnes, John; Levy, Colin; Leys, David; Whitehead, Roger C.; Stratford, Ian J.; Bryce, Richard A.
Journal of Medicinal Chemistry, 2009 , vol. 52, # 22 p. 7142 - 7156
反应条件
triethylamine in tetrahydrofuran T=80°C; P=7355.08 Torr; 4 h;
参考文献
Mizuno, Takumi; Nishiguchi, Ikuzo; Hirashima, Tsuneaki; Ogawa, Akiya; Kambe, Nobuaki; Sonoda, Noboru
Synthesis, 1988 , # 3 p. 257 - 259
反应条件
1: 33 percent / PhN(Me)MgBr / diethyl ether / 3 h / 20 °C 2: 84 percent / conc. HCl / 24 h / 20 °C 3: 54 percent / KOH / methanol / 0.5 h / Heating View Scheme
参考文献
Russian Chemical Bulletin, , vol. 49, # 3 p. 478 - 481
反应条件
1: potassium carbonate / acetone / |Inert atmosphere; |Reflux 2: sodium hydride / mineral oil / |Inert atmosphere; |Reflux 3: Ba(OH)2 / methanol; water / 2 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Organic Letters, , vol. 15, # 10 p. 2430 - 2433
反应条件
trichlorophosphate T=105°C; 4 h;
参考文献
Knierzinger; Wolfbeis
Journal of Heterocyclic Chemistry, 1980 , vol. 17, # 2 p. 225 - 229
反应条件
potassium hydroxide in methanol Hydrolysis; 0.5 h; Heating;
参考文献
Sosnovskikh; Kutsenko; Ovsyannikov
Russian Chemical Bulletin, 2000 , vol. 49, # 3 p. 478 - 481
反应条件
1: zinc(II) chloride / 5 h / |Inert atmosphere; |Reflux 2: potassium carbonate / acetone / |Inert atmosphere; |Reflux 3: sodium hydride / mineral oil / |Inert atmosphere; |Reflux 4: Ba(OH)2 / methanol; water / 2 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Organic Letters, , vol. 15, # 10 p. 2430 - 2433
反应条件
in xylene 2 h; Heating;
参考文献
Knierzinger; Wolfbeis
Journal of Heterocyclic Chemistry, 1980 , vol. 17, # 2 p. 225 - 229
参考文献
Chemische Berichte, , vol. 50, p. 1295
反应条件
1: 84 percent / conc. HCl / 24 h / 20 °C 2: 54 percent / KOH / methanol / 0.5 h / Heating View Scheme
参考文献
Russian Chemical Bulletin, , vol. 49, # 3 p. 478 - 481
