N-氯甲基邻苯二甲酰亚胺合成路线 (共 64 条)
反应条件
thionyl chloride in dichloromethane; N,N-dimethyl-formamide T=20°C; 2.5 h;
参考文献
Huang, Zhongyan; Xu, Jiaxi
Tetrahedron, 2013 , vol. 69, # 3 p. 1050 - 1056
反应条件
1: in water Heating; 2: With thionyl chloride in dichloromethane; N,N-dimethyl-formamide T=20°C; Further stages.;
参考文献
Cho, Su-Dong; Hwang, Jaeyoung; Kim, Ho-Kyun; Yim, Heung-Sup; Kim, Jeum-Jong; Lee, Sang-Gyeong; Yoon, Yong-Jin
Journal of Heterocyclic Chemistry, 2007 , vol. 44, # 4 p. 951 - 960
反应条件
tert-butylhypochlorite; Ag(Phen)2OTf in acetonitrile T=20°C; 18 h; Inert atmosphere;
参考文献
Wang, Zhentao; Zhu, Lin; Yin, Feng; Su, Zhongquan; Li, Zhaodong; Li, Chaozhong
Journal of the American Chemical Society, 2012 , vol. 134, # 9 p. 4258 - 4263
反应条件
1: H2O 2: PCl5 / diethyl ether View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 18 p. 4913 - 4918
反应条件
thionyl chloride in diethyl ether 24 h;
参考文献
Orlova, N.A.; Shipov, A.G.; Savost'yanova, I.A.; Baukov, Yu.I.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 9.2 p. 2024 - 2031,1875 - 1881
反应条件
zinc(II) chloride T=240°C;
参考文献
Chemische Berichte, , vol. 41, p. 248
反应条件
acetic anhydride; chlorine in tetrachloromethane 0.5 h; Ambient temperature; Yield given;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 28, # 1 p. 126 - 133
反应条件
sulfuryl dichloride; acetic anhydride in tetrachloromethane 0.5 h; Ambient temperature; Yield given;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 28, # 1 p. 126 - 133
反应条件
acetic anhydride; chlorine in tetrachloromethane 0.5 h; Ambient temperature; Yield given;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 28, # 1 p. 126 - 133
反应条件
sulfuryl dichloride; acetic anhydride in tetrachloromethane 1 h; Ambient temperature; Yield given;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 28, # 1 p. 126 - 133