1: NaN3 / H2O; acetone / 18 h / 0 °C 2: 99.0 g / benzene / 24 h / Heating View Scheme

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<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1209273', constants.ctx, '0')">thionyl chloride</a> <br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: 100 percent / 12 h / Ambient temperature<br />2: SOCl₂ / CHCl₃; dimethylformamide / 4 h / Heating<br /> <br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1: 93 percent / acetic anhydride / Heating<br />2: 100 percent / 12 h / Ambient temperature<br />3: SOCl₂ / CHCl₃; dimethylformamide / 4 h / Heating<br /> <br /> &nbsp;