2-(2,6-二氯苯基)硫代乙酰胺合成路线 (共 3 条)
反应条件
potassium carbonate in N,N-dimethyl-formamide T=80°C;
参考文献
Liu, Jing; Fitzgerald, Anne E.; Lebsack, Alec D.; Mani, Neelakandha S.
Organic Process Research and Development, 2011 , vol. 15, # 2 p. 382 - 388
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0); potassium tert-butylate in N,N-dimethyl-formamide T=70°C;
参考文献
Liu, Jing; Fitzgerald, Anne E.; Lebsack, Alec D.; Mani, Neelakandha S.
Organic Process Research and Development, 2011 , vol. 15, # 2 p. 382 - 388
反应条件
1: 30 percent / 100 °C 2: 93 percent / aq. KOH / tetrahydrofuran 3: oxalyl chloride / CHCl3 View Scheme
参考文献
Larsen, Scott D.; Stachew, Carl F.; Clare, Paula M.; Cubbage, Jerry W.; Leach, Karen L.
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 20 p. 3491 - 3495