1-[(2-氯苯基)硫]-2-丙酮合成路线 （共 3 条）
反应条件
potassium carbonate in acetone 2 h; Reflux;
参考文献
KANCERA AB; BYSTROeM, Styrbjoern; HEDGECOCK, Charles; HOMAN, Evert; LUNDBAeCK, Thomas; MARTINSSON, Jessica; SARI, Meral; FAeRNEGAaRDH, Katarina; JOeNSSON, Mattias
Patent: WO2012/35171 A2, 2012 ;
Location in patent: Page/Page column 47 ;
WO 2012/035171 A2
反应条件
PPA T=115 - 120°C; 4 h;
参考文献
KANCERA AB; BYSTROeM, Styrbjoern; HEDGECOCK, Charles; HOMAN, Evert; LUNDBAeCK, Thomas; MARTINSSON, Jessica; SARI, Meral; FAeRNEGAaRDH, Katarina; JOeNSSON, Mattias
Patent: WO2012/35171 A2, 2012 ;
Location in patent: Page/Page column 47-48 ;
WO 2012/035171 A2
反应条件
1: polyphosphoric acid / 4 h / 115 - 120 °C
2: aq. NaOH / CuCl / 45 h / 260 - 290 °C
View Scheme
参考文献
Chapman,N.B. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1972 , p. 1404 - 1407
