反应条件
1: 2-bromo-2-phenyl-1-ethene With magnesium in tetrahydrofuran
2 h; Inert atmosphere;
2: iso-propylmagnesium bromide With Nitrous oxide in tetrahydrofuran
T=0°C; 0.0833333 h; Schlenk technique;
3: With dilithium tetrachlorocuprate; isopropylmagnesium chloride in tetrahydrofuran
2 h; Schlenk technique;
参考文献
Kiefer, Gregor; Jeanbourquin, Loic; Severin, Kay
Angewandte Chemie - International Edition, 2013 , vol. 52, # 24 p. 6302 - 6305
Angew. Chem., 2013 , vol. 125, # 24 p. 6422 - 6425