(S)-(-)-N-苄基-1-苯基-乙胺合成路线 （共 37 条）
反应条件
1: 89 percent / NaHCO3, sodium iodide / tetrahydrofuran; dimethylsulfoxide / Heating 2: 85 percent / 2-mercaptobenzoic acid, Pd(dba)2, DPPB / tetrahydrofuran / 20 °C View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. 132, p. 1157 - 1166
反应条件
1: 89 percent / NaHCO3, sodium iodide / tetrahydrofuran; dimethylsulfoxide / Heating 2: 85 percent / 2-mercaptobenzoic acid, Pd(dba)2, DPPB / tetrahydrofuran / 20 °C View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. 132, p. 1157 - 1166
反应条件
1: 88 percent / 2-mercaptobenzoic acid, Pd(dba)2, DPPB / tetrahydrofuran / Ambient temperature 2: 89 percent / NaHCO3, sodium iodide / tetrahydrofuran; dimethylsulfoxide / Heating 3: 85 percent / 2-mercaptobenzoic acid, Pd(dba)2, DPPB / tetrahydrofuran / 20 °C View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. 132, p. 1157 - 1166
反应条件
1.1: / toluene / 4 h / 150 °C / 37503.8 Torr / Continuous flow recycle reactor 2.1: methanol / 2 h / 20 °C 2.2: 16 h / 20 - 28 °C 3.1: CHIRACEL OD-H / hexane; isopropylamine / Resolution of racemate View Scheme
参考文献
Green Chemistry, , vol. 14, # 1 p. 226 - 232
反应条件
CHIRACEL OD-H in hexane; isopropylamine Resolution of racemate;
参考文献
Green Chemistry, , vol. 14, # 1 p. 226 - 232
反应条件
1.1: methanol / 2 h / 20 °C 1.2: 16 h / 20 - 28 °C 2.1: CHIRACEL OD-H / hexane; isopropylamine / Resolution of racemate View Scheme
参考文献
Green Chemistry, , vol. 14, # 1 p. 226 - 232
反应条件
2: d-tartaric acid; water View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2>86, p. 284,287
反应条件
(2S,3S)-2,3-dihydroxybutanedioic acid; water
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2>86, p. 284,287
反应条件
2: d-tartaric acid; water View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2>86, p. 284,287
反应条件
2: d-tartaric acid; water View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2>86, p. 284,287
