2,3,5-三苯甲酰尿苷合成路线 （共 51 条）
反应条件
Bislt;trifluoromethylgt;mercury; copper in N,N-dimethyl acetamide T=140°C; 2 h;
参考文献
Nowak, Ireneusz; Robins, Morris J.
Journal of Organic Chemistry, 2007 , vol. 72, # 7 p. 2678 - 2681
反应条件
1: [131I]-Uracil With N,O-bis-(trimethylsilyl)-acetamide in acetonitrile T=20°C; 0.5 h; 2: 2,3,5-tri-O-benzoyl-D-ribofuranosyl(N-phenyl)trifluoroacetimidate With trimethylsilyl trifluoromethanesulfonate in 1,2-dichloro-ethane T=20°C; Further stages.;
参考文献
Liao, Jinxi; Sun, Jiansong; Yu, Biao
Tetrahedron Letters, 2008 , vol. 49, # 34 p. 5036 - 5038
反应条件
silver trifluoromethanesulfonate; diphenyltin sulfide in 1,2-dichloro-ethane; acetonitrile T=60°C; 6 h;
参考文献
Mukaiyama, Teruaki; Matsutani, Takafumi; Shimomura, Naoyuki
Chemistry Letters, 1993 , # 9 p. 1627 - 1630
反应条件
stannous iodide in acetonitrile T=60°C; 6 h;
参考文献
Mukaiyama, Teruaki; Nagai, Masashi; Matsutani, Takafumi; Shimomura, Naoyuki
Nucleosides and Nucleotides, 1996 , vol. 15, # 1-3 p. 17 - 30
反应条件
1: With N,O-bis(trimethylsilyl) trifluoroacetamide in acetonitrile T=20°C; 0.5 h; Inert atmosphere; 2: With Au(Ph3P)+NTf2- in acetonitrile T=20°C; 72 h; Inert atmosphere;
参考文献
Zhang, Qingju; Sun, Jiansong; Zhu, Yugen; Zhang, Fuyi; Yu, Biao
Angewandte Chemie - International Edition, 2011 , vol. 50, # 21 p. 4933 - 4936
反应条件
2,6-di-tert-butyl-4-methylpyridinium triflate in acetonitrile T=100°C; silyl-Hilbert-Johnson reaction; 0.333333 h; tubing reactor;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 9 p. 2155 - 2158
反应条件
silver trifluoromethanesulfonate; diphenyltin sulfide in acetonitrile T=60°C; 4 h;
参考文献
Shimomura; Matsutani; Mukaiyama
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 11 p. 3100 - 3106
反应条件
1: thioether-bound (4-hydroxypyrimidine-2-yl)-Merrifield resin With 2,3,5-trimethyl-pyridine; trimethylsilyl trifluoromethanesulfonate in dichloromethane T=0 - 20°C; 48 h; 2: 1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose With trimethylsilyl iodide T=0°C; 48 h; 3: With Oxonereg; in 1,4-dioxane; water 12 h; Heating;
参考文献
Petricci, Elena; Renzulli, Michela; Radi, Marco; Corelli, Federico; Botta, Maurizio
Tetrahedron Letters, 2002 , vol. 43, # 52 p. 9667 - 9670
反应条件
water in ethylene glycol dimethyl ether T=125°C; 12 h;
参考文献
Organic Letters, , vol. 7, # 22 p. 4903 - 4905
反应条件
water in ethylene glycol dimethyl ether T=125°C; 12 h;
参考文献
Organic Letters, , vol. 7, # 22 p. 4903 - 4905
