2-(2-氟苯基)-苯并噻唑合成路线 (共 14 条)
反应条件
tetrakis(triphenylphosphine) palladium(0); N-fluoro-N-(phenylsulfonyl)benzene-sulfonamide; L-proline in cyclohexane T=120°C; 5 h; Sealed tube; regioselective reaction;
参考文献
Ding, Qiuping; Ye, Changqing; Pu, Shouzhi; Cao, Banpeng
Tetrahedron, 2014 , vol. 70, # 2 p. 409 - 416
反应条件
tetrakis(triphenylphosphine) palladium(0); N-fluoro-N-(phenylsulfonyl)benzene-sulfonamide; L-proline in cyclohexane
T=120°C; 5 h; Sealed tube; regioselective reaction;
参考文献
Ding, Qiuping; Ye, Changqing; Pu, Shouzhi; Cao, Banpeng
Tetrahedron, 2014 , vol. 70, # 2 p. 409 - 416
反应条件
palladium diacetate
T=60 - 75°C; 12 h; Ionic liquid;
参考文献
Kalkhambkar, Rajesh G.; Laali, Kenneth K.
Tetrahedron Letters, 2012 , vol. 53, # 32 p. 4212 - 4215
反应条件
tetrakis(triphenylphosphine) palladium(0); N-fluoro-N-(phenylsulfonyl)benzene-sulfonamide; L-proline in cyclohexane
T=120°C; 5 h; Sealed tube; regioselective reaction;
参考文献
Ding, Qiuping; Ye, Changqing; Pu, Shouzhi; Cao, Banpeng
Tetrahedron, 2014 , vol. 70, # 2 p. 409 - 416
反应条件
oxygen; copper(II) sulfate in dimethyl sulfoxide
T=130°C; 24.5 h; Sealed tube;
参考文献
Song, Qiuling; Feng, Qiang; Zhou, Mingxin
Organic Letters, 2013 , vol. 15, # 23 p. 5990 - 5993
反应条件
in ethanol
8 h; Heating;
参考文献
Mashraqui, Sabir H.; Dhaval, Vashi; Subramanian; Khan, Tabrez B.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 3 p. 815 - 819
反应条件
tert.-butylhydroperoxide; potassium iodide in water
T=100°C; 8 h; Inert atmosphere;
参考文献
Gao, Yuyu; Song, Qiuling; Cheng, Guolin; Cui, Xiuling
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 7 p. 1044 - 1047
反应条件
1: in water; dimethyl sulfoxide
T=100°C; 1 h; Inert atmosphere;
2: With dipotassium peroxodisulfate
3 h; Inert atmosphere;
参考文献
Yang, Zhiyong; Chen, Xiang; Wang, Sizhuo; Liu, Jidan; Xie, Kai; Wang, Anwei; Tan, Ze
Journal of Organic Chemistry, 2012 , vol. 77, # 16 p. 7086 - 7091
反应条件
dipotassium peroxodisulfate; potassium tert-butylate in water; dimethyl sulfoxide
T=100°C; 8 h;
参考文献
Yang, Zhiyong; Wang, Anwei; Chen, Xiang; Gui, Qingwen; Liu, Jidan; Tan, Ze; Wang, Hua; Shi, Ji-Cheng
Synlett, 2013 , vol. 24, # 12 art. no. ST-2013-W0351-L, p. 1549 - 1554
反应条件
sodium hydroxide; potassium hexacyanoferrate(III)
参考文献
Roe,A.; Tucker,W.P.
Journal of Heterocyclic Chemistry, 1965 , vol. 2, p. 148 - 151