6,7-二甲氧基-1,2,3,4-四氢异喹啉合成路线 （共 60 条）
反应条件
1: Zn/Hg; HCl / ethanol 2: HCl / ethanol / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 10, # 1 p. 87 - 95
参考文献
Grieco, Paul A.; Clark, Jerry D.
Journal of Organic Chemistry, 1990 , vol. 55, # 8 p. 2271 - 2272
反应条件
1: 93 percent / aq. NaIO4 / methanol / 20 h / Ambient temperature 2: 68 percent / TFAA / benzene / 18 h / Ambient temperature 3: 76 percent / NaBH4, NiCl2*6H2O / methanol; tetrahydrofuran / 0.5 h / Ambient temperature 4: 78 percent / 10percent NaOH / ethanol / 18 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 45, # 5 p. 813 - 819
反应条件
1: 68 percent / TFAA / benzene / 18 h / Ambient temperature 2: 76 percent / NaBH4, NiCl2*6H2O / methanol; tetrahydrofuran / 0.5 h / Ambient temperature 3: 78 percent / 10percent NaOH / ethanol / 18 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 45, # 5 p. 813 - 819
反应条件
1: 76 percent / NaBH4, NiCl2*6H2O / methanol; tetrahydrofuran / 0.5 h / Ambient temperature 2: 78 percent / 10percent NaOH / ethanol / 18 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 45, # 5 p. 813 - 819
反应条件
1: 96 percent / aq. NaIO4 / methanol / 20 h / Ambient temperature 2: 97 percent / TFAA / benzene / 20 h / Ambient temperature 3: 74 percent / NaBH4, NiCl2*6H2O / methanol; tetrahydrofuran / 0.5 h / Ambient temperature 4: 100 percent / 10percent NaOH / ethanol / 4 h / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 45, # 5 p. 813 - 819
反应条件
1: 74 percent / NaBH4, NiCl2*6H2O / methanol; tetrahydrofuran / 0.5 h / Ambient temperature 2: 100 percent / 10percent NaOH / ethanol / 4 h / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 45, # 5 p. 813 - 819
反应条件
1: 97 percent / TFAA / benzene / 20 h / Ambient temperature 2: 74 percent / NaBH4, NiCl2*6H2O / methanol; tetrahydrofuran / 0.5 h / Ambient temperature 3: 100 percent / 10percent NaOH / ethanol / 4 h / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 45, # 5 p. 813 - 819
反应条件
1: 93 percent / aq. NaIO4 / methanol / 20 h / Ambient temperature 2: 64 percent / TFAA / benzene / 16 h / Ambient temperature 3: 59 percent / NaBH4, NiCl2*6H2O / methanol; tetrahydrofuran / 0.5 h / Ambient temperature 4: 89 percent / 10percent NaOH / ethanol / 18 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 45, # 5 p. 813 - 819
反应条件
1: 64 percent / TFAA / benzene / 16 h / Ambient temperature 2: 59 percent / NaBH4, NiCl2*6H2O / methanol; tetrahydrofuran / 0.5 h / Ambient temperature 3: 89 percent / 10percent NaOH / ethanol / 18 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 45, # 5 p. 813 - 819
