2,5-双(氯甲基)-1,4-双(辛氧基)苯合成路线 （共 6 条）
反应条件
hydrogenchloride in 1,4-dioxane; water T=60 - 70°C;
参考文献
Steuerman, David W.; Star, Alexander; Narizzano, Riccardo; Choi, Hyeon; Ries, Ryan S.; Nicolini, Claudio; Stoddart, J. Fraser; Heath, James R
Journal of Physical Chemistry B, 2002 , vol. 106, # 12 p. 3124 - 3130
反应条件
1: 71 percent / K2CO3 / dimethylformamide / 120 h / 90 °C 2: 77 percent / aq. HCl / dioxane / 9 h / 60 - 70 °C View Scheme
参考文献
Star, Alexander; Stoddart, J. Fraser; Steuerman, David; Diehl, Mike; Boukai, Akram; Wong, Eric W.; Yang, Xin; Chung, Sung-Wook; Choi, Hyeon; Heath, James R.
Angewandte Chemie - International Edition, 2001 , vol. 40, # 9 p. 1721 - 1725
反应条件
1: 71 percent / K2CO3 / dimethylformamide / 120 h / 90 °C 2: 77 percent / aq. HCl / dioxane / 9 h / 60 - 70 °C View Scheme
参考文献
Star, Alexander; Stoddart, J. Fraser; Steuerman, David; Diehl, Mike; Boukai, Akram; Wong, Eric W.; Yang, Xin; Chung, Sung-Wook; Choi, Hyeon; Heath, James R.
Angewandte Chemie - International Edition, 2001 , vol. 40, # 9 p. 1721 - 1725
反应条件
1: 82 percent / potassium iodide; Aliquat 336; sodium hydroxide / ethanol; H2O / 120 h / Heating 2: 68 percent / hydrogen chloride / dioxane; HCl / 2 h / Heating View Scheme
参考文献
Detert, Heiner; Schollmeyer, Dieter; Sugiono, Erli
European Journal of Organic Chemistry, 2001 , # 15 p. 2927 - 2938
参考文献
Detert, Heiner; Sugiono, Erli
Journal of Physical Organic Chemistry, 2000 , vol. 13, # 10 p. 587 - 590
参考文献
Detert, Heiner; Schollmeyer, Dieter; Sugiono, Erli
European Journal of Organic Chemistry, 2001 , # 15 p. 2927 - 2938
