(S)-(+)-5-己烯-2-醇合成路线 (共 51 条)
参考文献
Colonge; Lagier
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1947 , vol. 224, p. 572,573
Bulletin de la Societe Chimique de France, 1949 , p. 20,21
反应条件
D-glucose; Yarrowia lipolytica YL2; peptone in N,N-dimethyl-formamide T=28°C; Oxidation; 96 h; Microbiological reaction; Title compound not separated from byproducts;
参考文献
Fantin, Giancarlo; Fogagnolo, Marco; Medici, Alessandro; Pedrini, Paola; Fontana, Silvia
Tetrahedron Asymmetry, 2000 , vol. 11, # 11 p. 2367 - 2373
参考文献
Gardner; Perkin
Journal of the Chemical Society, 1907 , vol. 91, p. 851
反应条件
1: 87 percent / pyridine / 1 h / Ambient temperature
2: 55 percent / lithium bromide / tetrahydrofuran / 6 h / Heating
3: 25 percent / sodium nitrite, urea / dimethylformamide / 48 h / Ambient temperature
View Scheme
参考文献
Williams,J.R. et al.
Journal of Organic Chemistry, 1978 , vol. 43, p. 1271 - 1272
反应条件
1: 80 percent / pyridine / 2 h / 0 - 5 °C
2: H2O2, KOH / methanol; H2O / 1.) 0-5 deg C, 2.) room temperature
View Scheme
参考文献
Porter, N. A.; Zuraw, P. J.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1345 - 1348
反应条件
pyridine
1 h; Ambient temperature;
参考文献
Bowman, W. Russell; Brown, David S.; Burns, Catherine A.; Crosby, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 17 p. 2099 - 2106
反应条件
triethylamine in dichloromethane
参考文献
Sun, Li-Qiang; Zhao, Qian; Renduchintala, Kishore V.; Sarkunam, Kandhasamy; Nagalakshim, Pulicharla; Gillis, Eric P.; Scola, Paul Michael
Patent: US2014/127156 A1, 2014 ;
Location in patent: Page/Page column ;
反应条件
phosphorus pentachloride
ohne Loesungsmittel;
参考文献
Courtot; Pierron
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1930 , vol. 190, p. 1058
反应条件
pyridine; diethyl ether; phosphorus tribromide
参考文献
Williams,J.R. et al.
Journal of Organic Chemistry, 1978 , vol. 43, p. 1271 - 1272
反应条件
ozone
Behandeln des erhaltenen Ozonids mit Zink und Essigsaeure;
参考文献
Mosher; Preiss
Journal of the American Chemical Society, 1953 , vol. 75, p. 5605