(S)-(+)-5-己烯-2-醇合成路线 (共 51 条)
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 224, p. 572,573
Bulletin de la Societe Chimique de France, , p. 20,21
参考文献
Annales de Chimie (Cachan, France), , vol. <4>3, p. 171
反应条件
1: pyridine 2: 64 percent / dimethylformamide / 14 h 3: naphthalene-2-thiol / benzene-d6 / 0.08 h / 15 °C / Irradiation View Scheme
参考文献
Hartung; Gallou
Journal of Organic Chemistry, 1995 , vol. 60, # 21 p. 6706 - 6716
反应条件
anhydrous lithium acetate; tetrabutyl-ammonium chloride; lithium chloride; palladium diacetate in N,N-dimethyl-formamide 96 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Larock; Leung; Stolz-Dunn
Tetrahedron Letters, 1989 , vol. 30, # 48 p. 6629 - 6632
反应条件
iodine; sodium hydrogencarbonate; potassium iodide in water
参考文献
Gevaza, Yu. I.; Kupchik, I. P.; Staninets, V. I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1981 , vol. 17, # 1 p. 24 - 26
Khimiya Geterotsiklicheskikh Soedinenii, 1981 , # 1 p. 32 - 34
反应条件
anhydrous lithium acetate; tetrabutyl-ammonium chloride; lithium chloride; palladium diacetate in N,N-dimethyl-formamide 96 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Larock; Leung; Stolz-Dunn
Tetrahedron Letters, 1989 , vol. 30, # 48 p. 6629 - 6632
反应条件
1: 66 percent / pyridine / CH2Cl2 / -5 - 20 °C 2: dimethylsulfoxide / 3 h / 60 °C View Scheme
参考文献
LeBel,N.A.; Banucci,E.G.
Journal of Organic Chemistry, 1971 , vol. 36, p. 2440 - 2448
反应条件
1: pyridine; diethyl ether; phosphorus (III)-bromide 2: hydrogen bromide View Scheme
参考文献
Golmow
Zhurnal Obshchei Khimii, 1952 , vol. 22, p. 2132,2135;engl.Ausg.S.2187
反应条件
ytterbium(III) triflate T=120°C; Inert atmosphereIonic liquid;
参考文献
Dzudza, Alma; Marks, Tobin J.
Chemistry - A European Journal, 2010 , vol. 16, # 11 p. 3403 - 3422
参考文献
Courtot; Pierron
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1930 , vol. 190, p. 1058