(S)-2-乙酰胺基-4-硝基苯丙氨酸合成路线 （共 13 条）
反应条件
hydrogen; lt;Rh(1(S),5(S),6(S)-1,6-bis(diphenylphosphinoxy)spirolt;4.4gt;nonanegt;+ in methanol T=25°C; P=760 Torr; 0.166667 h;
参考文献
Chan; Hu; Pai; Lau; Jiang; Mi; Yan; Sun; Lou; Deng
Journal of the American Chemical Society, 1997 , vol. 119, # 40 p. 9570 - 9571
反应条件
sulfuric acid; nitric acid T=60°C; 0.5 h;
参考文献
Maity, Suman Kumar; Kumar, Ravi; Ambast, Deepak K. S.; Pal, Bipul; Haldar, Debasish
Journal of Materials Chemistry, 2012 , vol. 22, # 41 p. 22198 - 22203
反应条件
hydrogen; Rh[(R)-H8-BDPAB(COD)]BF4 in ethanol T=20°C; P=1551.44 Torr; 0.166667 h; Title compound not separated from byproducts;
参考文献
Zhang, Fu-Yao; Kwok, Wai Him; Chan, Albert S.C.
Tetrahedron Asymmetry, 2001 , vol. 12, # 16 p. 2337 - 2342
反应条件
hydrogenchloride; sodium hydroxide in water; acetic anhydride
参考文献
Rhone-Poulenc Rorer S.A.
Patent: US5969179 A1, 1999 ;
反应条件
sodium hydroxide in acetone 1 h;
参考文献
Garrido-Hernandez, Hugo; Moon, Kyung D.; Geahlen, Robert L.; Borch, Richard F.
Journal of Medicinal Chemistry, 2006 , vol. 49, # 11 p. 3368 - 3376
反应条件
bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate; C107H159NO9P2; hydrogen in methanol; cyclohexane T=20°C; P=45603.1 Torr; 3 h; Autoclave; optical yield given as percent eeenantioselective reaction;
参考文献
Yi, Bing; He, Hua-Ping; Fan, Qing-Hua
Journal of Molecular Catalysis A: Chemical, 2010 , vol. 315, # 1 p. 82 - 85
反应条件
Gewinnung ueber das Brucin-Salz;
参考文献
Easton, Christopher J.; Harper, Jason B.
Tetrahedron Letters, 1998 , vol. 39, # 29 p. 5269 - 5272
反应条件
1: aqueous Na2CO3 / anschliessend Behandeln mit wss. HCl 2: Gewinnung ueber das Brucin-Salz View Scheme
参考文献
Bergel et al.
Journal of the Chemical Society, 1955 , p. 1229
Org. Synth. Isotopes, 1958 , p. 303
反应条件
1: acetic acid anhydride; HNO3; NO2 2: aqueous Na2CO3 / anschliessend Behandeln mit wss. HCl 3: Gewinnung ueber das Brucin-Salz View Scheme
参考文献
Bergel et al.
Journal of the Chemical Society, 1955 , p. 1229
Org. Synth. Isotopes, 1958 , p. 303
反应条件
1: pyridine / 20 °C 2: sulfuric acid; nitric acid / 0.5 h / 60 °C View Scheme
参考文献
Maity, Suman Kumar; Kumar, Ravi; Ambast, Deepak K. S.; Pal, Bipul; Haldar, Debasish
Journal of Materials Chemistry, 2012 , vol. 22, # 41 p. 22198 - 22203
