2,2-双(三氟甲基)丙酰胺合成路线 (共 8 条)
反应条件
N-benzyl-N,N,N-triethylammonium chloride T=97 - 98°C; 2 h; var. phase transfer reag.: PhCH2Me3NCl, PhCH2Ph3NCl;
参考文献
Misaki, Susumu
Journal of Fluorine Chemistry, 1985 , vol. 29, p. 471 - 475
反应条件
triethylamine (heating);
参考文献
Cheburkov,Yu.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1964 , p. 339 - 341
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1964 , p. 367 - 369
反应条件
N,N-dimethyl-formamide T=130°C;
参考文献
Ohsaka, Yohnosuke; Amimoto, Yoshio; Takaki, Shoji
Journal of Fluorine Chemistry, 1982 , vol. 21, p. 54
参考文献
Rossman, D. I.; Muller, A. J.
Journal of Fluorine Chemistry, 1993 , vol. 60, # 1 p. 61 - 68
参考文献
Knunyants,I.L. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1966 , p. 985 - 991
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1966 , p. 1031 - 1038
反应条件
aluminium trichloride
参考文献
L Knunyants,I. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1966 , p. 992 - 999
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1966 , p. 1038 - 1047
反应条件
N,N-dimethyl-formamide
T=130°C;
参考文献
Ohsaka, Yohnosuke; Amimoto, Yoshio; Takaki, Shoji
Journal of Fluorine Chemistry, 1982 , vol. 21, p. 54
反应条件
(i) aq. NaOH, (ii) (heating in PhNO2); Multistep reaction;
参考文献
Knunyants,I.L. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1971 , vol. 20, p. 93 - 98
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1971 , vol. 20, # 1 p. 110 - 117