(E)-3-环己基-2-丙烯酸乙酯合成路线 (共 42 条)
反应条件
1: With potassium carbonate
Horner-Wadsworth-Emmons olefination; 6 h; Neat (no solvent)high-speed ball milling;
2: With Oxonereg;
12 h; Neat (no solvent)high-speed ball milling; optical yield given as percent dediastereoselective reaction;
参考文献
Shearouse, William C.; Korte, Chelsea M.; Mack, James
Green Chemistry, 2011 , vol. 13, # 3 p. 598 - 601
反应条件
(i) nBuLi, (ii) /BRN= 383571/; Multistep reaction;
参考文献
Gerkin,R.M.; Rickborn,B.
Journal of the American Chemical Society, 1967 , vol. 89, # 23 p. 5850 - 5855
反应条件
T=27°C; 336 h; Irradiation;
参考文献
Buechi,G.; Feairheller,S.H.
Journal of Organic Chemistry, 1969 , vol. 34, p. 609 - 612
反应条件
potassium tert-butylate
1.) THF, -20 deg C, 2.) -20 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Osuka, Atsuhiro; Mori, Yasuo; Shimizu, Hirohito; Suzuki, Hitomi
Tetrahedron Letters, 1983 , vol. 24, # 25 p. 2599 - 2602
反应条件
Yield given. Multistep reaction;
参考文献
Matui, Syuichi; Tanaka, Kazuhiko; Kaji, Aritsune
Synthesis, 1983 , # 2 p. 127 - 128
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Matsui, Syuichi
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 2 p. 426 - 434
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Matsui, Syuichi
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 2 p. 426 - 434
反应条件
triethylamine in cyclohexane
3.5 h; Irradiation;
参考文献
Buechi,G.; Feairheller,S.H.
Journal of Organic Chemistry, 1969 , vol. 34, p. 609 - 612
反应条件
diethylamine in dichloromethane
T=0°C; Irradiation;
参考文献
Piva, Olivier
Tetrahedron, 1994 , vol. 50, # 48 p. 13687 - 13696
反应条件
triethylamine in cyclohexane
3.5 h; Irradiation;
参考文献
Buechi,G.; Feairheller,S.H.
Journal of Organic Chemistry, 1969 , vol. 34, p. 609 - 612