氯甲酸-2,2,2-三氯乙酯合成路线 （共 61 条）
反应条件
pyridine in dichloromethane
反应条件
sulfuryl dichloride in 1,2-dichloro-ethane Heating;
参考文献
Synthesis, , p. 600 - 602
反应条件
ammonium hydroxide T=0°C;
参考文献
Organic Letters, , vol. 11, # 13 p. 2944 - 2947
反应条件
sodium carbonate in water; acetone T=0°C; 3.5 h;
参考文献
Mallams, Alan K.; Morton, James B.; Reichert, Paul
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2186 - 2208
反应条件
in tetrahydrofuran T=20°C; 20 h;
参考文献
Hanrahan, Jane R.; Mewett, Kenneth N.; Chebib, Mary; Burden, Peter M.; Johnston, Graham A.R.
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 19 p. 2389 - 2392
反应条件
ammonia; sodium hydrogencarbonate; potassium carbonate in methanol; dichloromethane; acetone
参考文献
Duan, Jingwu; King, Bryan W.; Decicco, Carl; Maduskuie JR., Thomas P.; Voss, Matthew E.
Patent: US2002/13341 A1, 2002 ;
US 20020013341 A1
反应条件
potassium carbonate in 1,2-dichloro-ethane
参考文献
John Wyeth and Brother Limited
Patent: US4360519 A1, 1982 ;
参考文献
American Cyanamid Company
Patent: US5482971 A1, 1996 ;
US 5482971 A
反应条件
sodium hydrogencarbonate; triethylamine in diethyl ether
反应条件
pyridine in tetrahydrofuran T=0 - 20°C; 1.5 h;
参考文献
Takeda Pharmaceutical Company Limited
Patent: EP1813606 A1, 2007 ;
Location in patent: Page/Page column 51 ;
