反应条件
1: 96 percent / diisobutylaluminium hydride / diethyl ether; hexane / 1) -78 deg C to room temperature, 2) room temperature, 8 h
2: 91.3 percent / N-bromosuccinimide, Me2S / CH2Cl2 / 1) -30 deg C, 3 h, 2) room temperature, 1 h
3: 44.7 percent / m-chloroperbenzoic acid / CH2Cl2 / 1) 0 deg C, 1 h, 2) room temperature, 12 h
4: 33 percent / Bu3SnH, azoisobutyronitrile / benzene / 15 h / Heating
View Scheme
参考文献
Murphy, John A.; Patterson, Christopher W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 4 p. 405 - 410
