diisobutylaluminium hydride in diethyl ether; hexane 1) -78 deg C to room temperature, 2) room temperature, 8 h;
参考文献
Murphy, John A.; Patterson, Christopher W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 4 p. 405 - 410
1: NaBH4 / methanol / Ambient temperature
2: toluene-p-sulfonic acid / toluene / 4 h / Heating
View Scheme
参考文献
Murphy, John A.; Patterson, Christopher W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 4 p. 405 - 410
1: 51.4 percent / NaBH4 / ethanol / 6 h
3: NaBH4 / methanol / Ambient temperature
4: toluene-p-sulfonic acid / toluene / 4 h / Heating
View Scheme
参考文献
Murphy, John A.; Patterson, Christopher W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 4 p. 405 - 410
2: NaBH4 / methanol / Ambient temperature
3: toluene-p-sulfonic acid / toluene / 4 h / Heating
View Scheme
参考文献
Murphy, John A.; Patterson, Christopher W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 4 p. 405 - 410