1.1: NaH / dimethylformamide; various solvent(s) / 0.25 h / 20 °C
1.2: 71 percent / dimethylformamide; various solvent(s) / 48 h / 80 °C
2.1: 68 percent / aq. NaOH / ethanol / 3.5 h / Heating
View Scheme
参考文献
Fox, David J.; Pedersen, Daniel Sejer; Warren, Stuart
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 16 p. 3102 - 3107
1: oxyde de diphenylphosphinomethylephenylcetone With sodium methylate in tetrahydrofuran
T=20°C; 0.25 h;
2: α-bromoacetophenone in tetrahydrofuran
T=20°C; 27 h; Further stages.;
参考文献
Fox, David J.; Pedersen, Daniel Sejer; Warren, Stuart
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 16 p. 3102 - 3107
