6-氨基-2-甲基-4(3H)-喹唑啉酮合成路线 （共 3 条）
反应条件
hydrogen; palladium 10 on activated carbon in tetrahydrofuran; methanol 2.5 h;
参考文献
BRISTOL-MYERS SQUIBB COMPANY
Patent: WO2008/79759 A1, 2008 ;
Location in patent: Page/Page column 133-134 ;
WO 2008/079759 A1
反应条件
1: 95 percent / nitric acid / H2SO4 2: 87 percent / sodium sulphide / H2O / 2 h / Heating View Scheme
参考文献
Naik; Desai
Journal of the Indian Chemical Society, 1989 , vol. 66, # 7 p. 495 - 497
反应条件
1: 2.) liq. NH3 / 1.) reflux, 30 min; 2.) 100 deg C, 2 h 2: 95 percent / nitric acid / H2SO4 3: 87 percent / sodium sulphide / H2O / 2 h / Heating View Scheme
参考文献
Naik; Desai
Journal of the Indian Chemical Society, 1989 , vol. 66, # 7 p. 495 - 497
