[4-[2-(二甲基氨基)乙氧基]苯基](4-羟基苯基)甲酮合成路线 (共 4 条)
反应条件
1: 1.) 95percent potassium t-butoxide, n-butyllithium, TMEDA / 1.) hexane, r.t., 30 min; 2.) Et2O, -70 deg C to r.t., 3 h 2: 32percent H2SO4 / 16 h / 50 °C View Scheme
参考文献
Olier-Reuchet, Chantal; Aitken, David J.; Bucourt, Robert; Husson, Henri-Philippe
Tetrahedron Letters, 1995 , vol. 36, # 45 p. 8221 - 8224
反应条件
titanium tetrachloride; zinc in tetrahydrofuran 5 h; Heatingother reagents: TiCl3, Li; Yield given. Yields of byproduct given;
参考文献
Gauthier, Sylvain; Mailhot, Josee; Labrie, Fernand
Journal of Organic Chemistry, 1996 , vol. 61, # 11 p. 3890 - 3893
反应条件
titanium tetrachloride; zinc in tetrahydrofuran 5 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 61, # 11 p. 3890 - 3893
反应条件
titanium tetrachloride; zinc in tetrahydrofuran 5 h; Heatingother reagents: TiCl3, Li; Yield given. Yields of byproduct given;
参考文献
Gauthier, Sylvain; Mailhot, Josee; Labrie, Fernand
Journal of Organic Chemistry, 1996 , vol. 61, # 11 p. 3890 - 3893