in toluene byproducts: H2O; mixt. of (Bu3Sn)2O and PhSH (1:2 molar ratio) refluxed (12 h) in toluenewith removal of H2O (Dean-Stark apparatus); toluene removed (vac.); residue distd. (vac.);
参考文献
Sutton, Andrew D.; Davis, Benjamin L.; Bhattacharyya, Koyel X.; Ellis, Bobby D.; Gordon, John C.; Power, Philip P.
Chemical Communications, 2010 , vol. 46, # 1 p. 148 - 149
Sutton, Andrew D.; Davis, Benjamin L.; Bhattacharyya, Koyel X.; Ellis, Bobby D.; Gordon, John C.; Power, Philip P.
Chemical Communications, 2010 , vol. 46, # 1 p. 148 - 149
→
反应条件
in not given byproducts: LiCl;
参考文献
Strohmann; Abele
Angewandte Chemie - International Edition in English, 1996 , vol. 35, # 20 p. 2378 - 2380