6-甲氧基-1,2,3,4-四氢萘合成路线 (共 69 条)
反应条件
tert.-butylhydroperoxide; sodium hydrogencarbonate; cis-(2,2)-Rh2(cap)4 in decane; 1,2-dichloro-ethane T=20°C; 16 h; Title compound not separated from byproducts;
参考文献
Catino, Arthur J.; Nichols, Jason M.; Choi, Hojae; Gottipamula, Sidhartha; Doyle, Michael P.
Organic Letters, 2005 , vol. 7, # 23 p. 5167 - 5170
反应条件
1: CrO3; aqueous H2SO4 View Scheme
参考文献
Miki
Yakugaku Zasshi, 1941 , vol. 61, p. 272,278
Full Text Show Details
Riedel A.G.
Patent: DE397150 , 1920 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 460
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane T=60°C; 24 h; DDQ/substrate ratio = 2;
参考文献
Lemaire, Marc; Doussot, Joel; Guy, Alain
Chemistry Letters, 1988 , # 10 p. 1581 - 1584
反应条件
1: Me3SiN3, DDQ / CHCl3 / 96 h / Ambient temperature 2: H2 / Pd-BaSO4 (5percent) / ethanol / 4 h / 760 Torr / Ambient temperature View Scheme
参考文献
Guy, Alain; Lemor, Alain; Doussot, Joel; Lemaire, Marc
Synthesis, 1988 , # 11 p. 900 - 902
反应条件
zirconium tetrachloride in dichloromethane 48 h; other substituted 6-methoxytetralins, ultrasonic irradiation, other reagents: TiCl4, ZrBr4, HfCl4, HfBr4, other solvents, presence of LiCl, Et2NH, EtSH, Bu4NBr, Bu4NBF4, Adogen 464, Aliquat 336, 18-crown-6, various reaction time; MechanismProduct distribution;
参考文献
Harrowven, David C.; Dainty, Richard F.
Tetrahedron, 1997 , vol. 53, # 46 p. 15771 - 15786
反应条件
oxygen; 9,10-anthracenedicarbonitrile; dimethyl viologen; iron(II) chloride in methanol; acetonitrile 2 h; Ambient temperatureIrradiation;
参考文献
Santamaria, Jean; Jroundi, Rachid
Tetrahedron Letters, 1991 , vol. 32, # 34 p. 4291 - 4294
反应条件
tert.-butylhydroperoxide; chromium(VI) oxide in dichloromethane 9 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 28, # 19 p. 2131 - 2132
反应条件
tert.-butylhydroperoxide; sodium hydrogencarbonate; cis-(2,2)-Rh2(cap)4 in decane; 1,2-dichloro-ethane T=20°C; 16 h; Title compound not separated from byproducts;
参考文献
Catino, Arthur J.; Nichols, Jason M.; Choi, Hojae; Gottipamula, Sidhartha; Doyle, Michael P.
Organic Letters, 2005 , vol. 7, # 23 p. 5167 - 5170
反应条件
dipotassium peroxodisulfate; anhydrous copper sulphate in water; acetonitrile T=65 - 70°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 22, # 27 p. 2605 - 2608
反应条件
ammonium cerium(IV) nitrate in methanol 0.0833333 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 47, # 9 p. 1647 - 1652