6-甲氧基-1,2,3,4-四氢萘合成路线 (共 69 条)
反应条件
hydrogen; polymer incarcerated palladium in ethanol T=50°C; P=53200 Torr; 18 h;
参考文献
Journal of Organic Chemistry, , vol. 69, # 8 p. 2871 - 2873
反应条件
palladium dichloride in methanol T=40°C; 24 h; Inert atmosphereGreen chemistry; chemoselective reaction;
参考文献
Wang, Hu; Li, Li; Bai, Xing-Feng; Shang, Jun-Yan; Yang, Ke-Fang; Xu, Li-Wen
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 2-3 p. 341 - 347
反应条件
palladium dichloride in methanol T=40°C; 24 h; Inert atmosphereGreen chemistry;
参考文献
Wang, Hu; Li, Li; Bai, Xing-Feng; Deng, Wen-Hui; Zheng, Zhan-Jiang; Yang, Ke-Fang; Xu, Li-Wen
Green Chemistry, 2013 , vol. 15, # 9 p. 2349 - 2355
反应条件
sodium hydroxide in ethanol 5 h; Heating;
参考文献
Mallory, Frank B.; Rudolph, M. Jonathan; Oh, Soon M.
Journal of Organic Chemistry, 1989 , vol. 54, # 19 p. 4619 - 4626
反应条件
Fuller's Earth; nickel; decalin T=60°C; P=18387.7 - 40452.9 Torr; Hydrogenation;
参考文献
US1918648 , ;
DE545195 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 822
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; Cooling with acetone-dry ice; 2: With boron triethoxide in tetrahydrofuran; hexane T=-78°C; 2 h; 3: With hydrogenchloride in tetrahydrofuran; hexane; water
参考文献
WO2003/91225 A1, ;
Page/Page column 56-57 ;
WO 03/091225 A1
反应条件
amberlyst 15 in chlorobenzene T=200°C; 3 h;
参考文献
Byung, Hyun Kim; Jong, Gil Lee; Woon, Ki Kim; Young, Gyu Kim
Organic Process Research and Development, 2005 , vol. 9, # 6 p. 814 - 817
反应条件
Raney Ni (W-2) in ethanol Heating;
参考文献
Rigby, James H.; Kotnis, Atul; Kramer, James
Tetrahedron Letters, 1983 , vol. 24, # 29 p. 2939 - 2940
反应条件
palladium dichloride in methanol T=40°C; 18 h; Inert atmosphereGreen chemistry; chemoselective reaction;
参考文献
Wang, Hu; Li, Li; Bai, Xing-Feng; Shang, Jun-Yan; Yang, Ke-Fang; Xu, Li-Wen
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 2-3 p. 341 - 347
反应条件
1: 77 percent / p-toluenesulfonic acid / acetonitrile / 24 h / 0 °C 2: 95 percent / Raney Ni (W-2) View Scheme
参考文献
Tetrahedron Letters, , vol. 24, # 29 p. 2939 - 2940