反应条件
1: 61 percent / sulfuryl chloride / CCl4 / 12 h / Ambient temperature
2: 91 percent / LiBr, Li2Co3 / dimethylformamide / 24 h / 100 °C
3: 93 percent / DIBAL-H / benzene; toluene / 2 h / 5 °C
4: 1.) BH3*THF, 2.) 3 M NaOH, 30 percent H2O2 / 1.) THF, 24 h, room temp. 2.) THF, water
5: 85 percent / K2Cr2O7-H2SO4 / acetone
View Scheme
参考文献
D'Haenens, L.; Sande, C. C. Van de; Tavernier, D.; Vandewalle, M.
Bulletin des Societes Chimiques Belges, 1986 , vol. 95, # 4 p. 273 - 282
