1-甲氧基-1,3,5-环庚三烯合成路线 （共 15 条）
反应条件
hydrogenchloride in methanol
参考文献
The United States of America as represented by the Secretary of the Army
Patent: US4249025 A1, 1981 ;
参考文献
Shono, Tatsuya; Nozoe, Tetsuo; Maekawa, Hirofumi; Yamaguchi, Yoshihide; Kanetaka, Shinya; Masuda, Haruhisa; Okada, Toshio; Kashimura, Shigenori
Tetrahedron, 1991 , vol. 47, # 4-5 p. 593 - 603
反应条件
1: 71 percent / Et4NOTs, NaOMe / -10 - 0 °C / carbon rod electrodes, 5 A, 3F/mol 2: 98 percent / 1 h / 150 °C 3: 85 percent / 5 h / 170 °C View Scheme
参考文献
Shono, Tatsuya; Nozoe, Tetsuo; Maekawa, Hirofumi; Yamaguchi, Yoshihide; Kanetaka, Shinya; Masuda, Haruhisa; Okada, Toshio; Kashimura, Shigenori
Tetrahedron, 1991 , vol. 47, # 4-5 p. 593 - 603
参考文献
Mueller,E. et al.
Justus Liebigs Annalen der Chemie, 1964 , vol. 675, p. 63 - 73
反应条件
1: 98 percent / Heating 2: 82 percent / Heating View Scheme
参考文献
Shono, Tatsuya; Nozoe, Tetsuo; Maekawa, Hirofumi; Yamaguchi, Yoshihide; Kanetaka, Shinya; Masuda, Haruhisa; Okada, Toshio; Kashimura, Shigenori
Tetrahedron, 1991 , vol. 47, # 4-5 p. 593 - 603
反应条件
(i) Br2, MeOH, (ii) /BRN= 3592982/, DMSO; Multistep reaction;
参考文献
Garbisch,E.W.
Journal of Organic Chemistry, 1965 , vol. 30, # 7 p. 2109 - 2120
反应条件
2: 10percent aq. H2SO4 3: H2 / 5percent Pd/C View Scheme
参考文献
Shono, Tatsuya; Nozoe, Tetsuo; Yamaguchi, Yoshihide; Ishifune, Manabu; Sakaguchi, Masashi; et al.
Tetrahedron Letters, 1991 , vol. 32, # 8 p. 1051 - 1054
反应条件
2: 1.) pyridinium bromide perbromide 2.) LiCl/LiCO3 / 2.) DMF 3: 100 percent / NH2NH2 4: 100 percent / KOH View Scheme
参考文献
Shono, Tatsuya; Nozoe, Tetsuo; Yamaguchi, Yoshihide; Ishifune, Manabu; Sakaguchi, Masashi; et al.
Tetrahedron Letters, 1991 , vol. 32, # 8 p. 1051 - 1054
反应条件
oxygen; hematoporphyrin IX in acetone 48 h; Irradiation;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 53, # 1 p. 236 - 238
反应条件
1: 85 percent / MeONa / -10 - 0 °C / anodic oxidation 2: 85 percent / H3O(+) View Scheme
参考文献
Tetrahedron Letters, , vol. 29, # 5 p. 555 - 558
