2-氰基苯硼酸 1,3-丙二醇酯合成路线 （共 29 条）
反应条件
K3PO4; Pd(PPh3)2Cl2 in toluene T=100°C; 12 h; Schlenk techniqueInert atmosphere;
参考文献
Organic Letters, , vol. 15, # 11 p. 2742 - 2745
反应条件
1: Pd(PPh3)2Cl2; K3PO4 / toluene / 12 h / 100 °C / |Schlenk technique; |Inert atmosphere 2: water; silver trifluoroacetate; dichloro bis(acetonitrile) palladium(II) / trifluoroacetic acid; N,N-dimethyl acetamide / 72 h / 140 °C / |Glovebox; |Inert atmosphere View Scheme
参考文献
Wan, Jung-Chih; Huang, Jun-Min; Jhan, Yu-Huei; Hsieh, Jen-Chieh
Organic Letters, 2013 , vol. 15, # 11 p. 2742 - 2745
反应条件
1: Pd(PPh3)2Cl2; K3PO4 / toluene / 12 h / 100 °C / |Schlenk technique; |Inert atmosphere 2: water; silver trifluoroacetate; dichloro bis(acetonitrile) palladium(II) / trifluoroacetic acid; N,N-dimethyl acetamide / 72 h / 140 °C / |Glovebox; |Inert atmosphere View Scheme
参考文献
Wan, Jung-Chih; Huang, Jun-Min; Jhan, Yu-Huei; Hsieh, Jen-Chieh
Organic Letters, 2013 , vol. 15, # 11 p. 2742 - 2745
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium phosphate in toluene 1 h; Heating;
参考文献
Urawa, Yoshio; Naka, Hiroyuki; Miyazawa, Mamoru; Souda, Shigeru; Ogura, Katsuyuki
Journal of Organometallic Chemistry, 2002 , vol. 653, # 1-2 p. 269 - 278
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium phosphate in toluene 1 h; Heating;
参考文献
Urawa, Yoshio; Naka, Hiroyuki; Miyazawa, Mamoru; Souda, Shigeru; Ogura, Katsuyuki
Journal of Organometallic Chemistry, 2002 , vol. 653, # 1-2 p. 269 - 278
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium phosphate in toluene 1 h; Heating;
参考文献
Urawa, Yoshio; Naka, Hiroyuki; Miyazawa, Mamoru; Souda, Shigeru; Ogura, Katsuyuki
Journal of Organometallic Chemistry, 2002 , vol. 653, # 1-2 p. 269 - 278
反应条件
K3PO4; Pd(PPh3)2Cl2 in toluene T=100°C; 12 h; Schlenk techniqueInert atmosphere;
参考文献
Wan, Jung-Chih; Huang, Jun-Min; Jhan, Yu-Huei; Hsieh, Jen-Chieh
Organic Letters, 2013 , vol. 15, # 11 p. 2742 - 2745
反应条件
K3PO4; Pd(PPh3)2Cl2 in toluene T=100°C; 12 h; Schlenk techniqueInert atmosphere;
参考文献
Wan, Jung-Chih; Huang, Jun-Min; Jhan, Yu-Huei; Hsieh, Jen-Chieh
Organic Letters, 2013 , vol. 15, # 11 p. 2742 - 2745
反应条件
1: Pd(PPh3)2Cl2; K3PO4 / toluene / 12 h / 100 °C / |Schlenk technique; |Inert atmosphere 2: palladium diacetate; water; zinc oxide / trifluoroacetic acid / 24 h / 120 °C View Scheme
参考文献
Wan, Jung-Chih; Huang, Jun-Min; Jhan, Yu-Huei; Hsieh, Jen-Chieh
Organic Letters, 2013 , vol. 15, # 11 p. 2742 - 2745
反应条件
1: Pd(PPh3)2Cl2; K3PO4 / toluene / 12 h / 100 °C / |Schlenk technique; |Inert atmosphere 2: palladium diacetate; water; silver trifluoroacetate / trifluoroacetic acid; N,N-dimethyl acetamide / 24 h / 160 °C View Scheme
参考文献
Wan, Jung-Chih; Huang, Jun-Min; Jhan, Yu-Huei; Hsieh, Jen-Chieh
Organic Letters, 2013 , vol. 15, # 11 p. 2742 - 2745
