2-氰基苯硼酸 1,3-丙二醇酯合成路线 （共 29 条）
参考文献
Universal Display Corporation
Patent: EP2243785 A1, 2010 ;
反应条件
caesium carbonate; palladium dichloride in N,N-dimethyl-formamide T=80°C; Suzuki-Miyaura Coupling; 6 h; Inert atmosphere;
参考文献
Journal of Medicinal Chemistry, , vol. 55, # 23 p. 10584 - 10600
反应条件
1: Pd(PPh3)2Cl2; K3PO4 / toluene / 12 h / 100 °C / |Schlenk technique; |Inert atmosphere 2: water; silver trifluoroacetate; dichloro bis(acetonitrile) palladium(II) / trifluoroacetic acid; N,N-dimethyl acetamide / 72 h / 140 °C / |Glovebox; |Inert atmosphere View Scheme
参考文献
Wan, Jung-Chih; Huang, Jun-Min; Jhan, Yu-Huei; Hsieh, Jen-Chieh
Organic Letters, 2013 , vol. 15, # 11 p. 2742 - 2745
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium phosphate in toluene T=110°C; Suzuki-Miyaura coupling recation; 4 h; Product distribution; Further Variations:ReagentsSolvents;
参考文献
Urawa, Yoshio; Ogura, Katsuyuki
Tetrahedron Letters, 2003 , vol. 44, # 2 p. 271 - 273
反应条件
pyridine; water; copper diacetate in N,N-dimethyl-formamide T=30°C; 24 h; KineticsProduct distribution; Further Variations:Reaction partnersamount of water;
参考文献
Nishiura, Katsutoshi; Urawa, Yoshio; Soda, Shigeru
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1679 - 1684
反应条件
pyridine; water; copper diacetate in N,N-dimethyl-formamide T=30°C; 24 h; KineticsProduct distribution; Further Variations:Reaction partnersamount of water;
参考文献
Nishiura, Katsutoshi; Urawa, Yoshio; Soda, Shigeru
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1679 - 1684
反应条件
K3PO4; Pd(PPh3)2Cl2 in toluene T=100°C; 12 h; Schlenk techniqueInert atmosphere;
参考文献
Wan, Jung-Chih; Huang, Jun-Min; Jhan, Yu-Huei; Hsieh, Jen-Chieh
Organic Letters, 2013 , vol. 15, # 11 p. 2742 - 2745
反应条件
1: Pd(PPh3)2Cl2; K3PO4 / toluene / 12 h / 100 °C / |Schlenk technique; |Inert atmosphere 2: palladium diacetate; water; silver trifluoroacetate / trifluoroacetic acid; N,N-dimethyl acetamide / 24 h / 160 °C 3: water; silver trifluoroacetate; dichloro bis(acetonitrile) palladium(II) / trifluoroacetic acid; N,N-dimethyl acetamide / 72 h / 160 °C View Scheme
参考文献
Wan, Jung-Chih; Huang, Jun-Min; Jhan, Yu-Huei; Hsieh, Jen-Chieh
Organic Letters, 2013 , vol. 15, # 11 p. 2742 - 2745
反应条件
1: Pd(PPh3)2Cl2; K3PO4 / toluene / 12 h / 100 °C / |Schlenk technique; |Inert atmosphere 2: water; silver trifluoroacetate; dichloro bis(acetonitrile) palladium(II) / trifluoroacetic acid; N,N-dimethyl acetamide / 72 h / 140 °C / |Glovebox; |Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 15, # 11 p. 2742 - 2745
反应条件
1: Pd(PPh3)2Cl2; K3PO4 / toluene / 12 h / 100 °C / |Schlenk technique; |Inert atmosphere 2: water; silver trifluoroacetate; dichloro bis(acetonitrile) palladium(II) / trifluoroacetic acid; N,N-dimethyl acetamide / 68 h / 140 °C / |Glovebox; |Inert atmosphere View Scheme
参考文献
Wan, Jung-Chih; Huang, Jun-Min; Jhan, Yu-Huei; Hsieh, Jen-Chieh
Organic Letters, 2013 , vol. 15, # 11 p. 2742 - 2745
