in further solvent(s) byproducts: LiCl, isobutylene; NaAlH4, dec-1-ene loaded in a vertical-type ball mill under Ar or N2; mixt. agitated for 10 min at 70°C; (i-Bu)2AlCl added for 0.5 h; mixt. stored for 1.5 h at 95-100°C; isobutylene collected in a trap cooled with liq. N2; ppt. sepd.; filtrate heated for 1 h at 80°C (1 Torr); elem. anal.;

triethylaluminum in hexane (N2); heating (autoclave, 140°C, 30 min, 120°C, 6 h); distn.; elem. anal.;

in toluene T=60°C; 6 h; oth. solvent, oth. temperature, oth. time; Product distribution;

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in toluene T=60°C; 6 h; oth. solvent, oth. temperature, oth. time; Product distribution;

dilithium tetrachlorocuprate; triphenylphosphine in octane T=50°C; 5 h;

in dichloromethane T=25°C; Yield given. Yields of byproduct given;