1-氧杂环十四烷-2-酮合成路线 （共 44 条）
反应条件
1.1: N,O-dimethylhydroxylamine hydrochloride; methyllithium / tetrahydrofuran / 0 - 20 °C
1.2: tetrahydrofuran / 0 - 20 °C
2.1: 2.54 g / imidazole / tetrahydrofuran / 2 h
3.1: tetrahydrofuran / 0 - 20 °C
View Scheme
参考文献
Muller, Thierry; Coowar, Djalil; Hanbali, Mazen; Heuschling, Paul; Luu, Bang
Tetrahedron, 2006 , vol. 62, # 51 p. 12025 - 12040
反应条件
1.1: N,O-dimethylhydroxylamine hydrochloride; methyllithium / tetrahydrofuran / 0 - 20 °C
1.2: tetrahydrofuran / 0 - 20 °C
2.1: 2.54 g / imidazole / tetrahydrofuran / 2 h
View Scheme
参考文献
Muller, Thierry; Coowar, Djalil; Hanbali, Mazen; Heuschling, Paul; Luu, Bang
Tetrahedron, 2006 , vol. 62, # 51 p. 12025 - 12040
反应条件
1.1: N,O-dimethylhydroxylamine hydrochloride; methyllithium / tetrahydrofuran / 0 - 20 °C
1.2: tetrahydrofuran / 0 - 20 °C
2.1: 2.54 g / imidazole / tetrahydrofuran / 2 h
3.1: tetrahydrofuran / 0 - 20 °C
4.1: 0.98 g / tetrabutylammonium fluoride / tetrahydrofuran / 15 h
View Scheme
参考文献
Muller, Thierry; Coowar, Djalil; Hanbali, Mazen; Heuschling, Paul; Luu, Bang
Tetrahedron, 2006 , vol. 62, # 51 p. 12025 - 12040
反应条件
1.1: N,O-dimethylhydroxylamine hydrochloride; methyllithium / tetrahydrofuran / 0 - 20 °C
1.2: tetrahydrofuran / 0 - 20 °C
2.1: 2.54 g / imidazole / tetrahydrofuran / 2 h
3.1: tetrahydrofuran / 0 - 20 °C
4.1: 0.98 g / tetrabutylammonium fluoride / tetrahydrofuran / 15 h
5.1: 76 percent / sodium hydride / tetrahydrofuran / Heating
View Scheme
参考文献
Muller, Thierry; Coowar, Djalil; Hanbali, Mazen; Heuschling, Paul; Luu, Bang
Tetrahedron, 2006 , vol. 62, # 51 p. 12025 - 12040
